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dc.contributor.authorAlyar, Saliha
dc.contributor.authorOzbek, Neslihan
dc.contributor.authorIskeleli, Nazan Ocak
dc.contributor.authorKaracan, Nurcan
dc.date.accessioned2019-11-24T20:35:27Z
dc.date.available2019-11-24T20:35:27Z
dc.date.issued2013
dc.identifier.issn1054-2523
dc.identifier.issn1554-8120
dc.identifier.urihttps://dx.doi.org/10.1007/s00044-012-0171-2
dc.identifier.urihttps://hdl.handle.net/20.500.12513/1850
dc.descriptionWOS: 000316912800001en_US
dc.description.abstractCopper(II) complexes of new aryldisulfonamides (L (1) = N,N'-bis[(2-methylphenyl)sulfonyl]ethylenediamine) and L (2) = N,N'-propanediyl-bis-benzenesulfonamide with 1,10-phenanthroline have been synthesized and characterized by using elemental analyses, FT-IR, LCMS, conductivity, and magnetic susceptibility techniques. The structures of [Cu(phen)(2)]L-1 (1) and [CuL2(phen)(2)] (2) compounds have been determined. Complex (1) has also been characterized by single crystal X-ray diffraction. The complex (1) crystallizes in the triclinic system, space group P1, with cell constants a = 12.9353(8) , b = 13.8543(9) , c = 14.4513(10) , alpha = 103.593(5)A degrees, beta A = 113.713(5)A degrees, gamma A = 106.104(5)A degrees, and Z = 1. The antibacterial activities of synthesized compounds were studied against Gram-positive bacteria: Staphylococcus aureus, Bacillus subtilis, and B. cereus and Gram-negative bacteria: Escherichia coli, Pseudomonas aeruginosa, and Yersinia enterocolitica by microdilution (as MICs in mu g/mL) and disk diffusion (as diameter zone in mm) method. The biological activity screening showed that (1) has more activity than (2) against the tested bacteria.en_US
dc.description.sponsorshipTUBITAKTurkiye Bilimsel ve Teknolojik Arastirma Kurumu (TUBITAK) [TBAG 104 T 390]; Gazi University Scientific Research ProjectsGazi University [05/2008-05]en_US
dc.description.sponsorshipThe authors wish to thank TUBITAK for the financial support (No: TBAG 104 T 390) and Gazi University Scientific Research Projects (No: 05/2008-05). We would also like to thank TUBITAK for the allocation of time for the NMR, Mass Spectra, and Elemental Analyses.en_US
dc.language.isoengen_US
dc.publisherSPRINGER BIRKHAUSERen_US
dc.relation.isversionof10.1007/s00044-012-0171-2en_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectSulfonamide Cu(II) complexesen_US
dc.subjectAntimicrobial activityen_US
dc.subjectDisk diffusion methoden_US
dc.subjectMICsen_US
dc.titleSynthesis, characterization, and antimicrobial activity of copper(II) complexes with N,N '-propanediyl-bis-benzenesulfonamide and N,N '-ethanediyl-bis-2-methylbenzenesulfonamideen_US
dc.typearticleen_US
dc.relation.journalMEDICINAL CHEMISTRY RESEARCHen_US
dc.contributor.departmentKırşehir Ahi Evran Üniversitesi, Eğitim Fakültesi, İlköğretim Bölümüen_US
dc.identifier.volume22en_US
dc.identifier.issue5en_US
dc.identifier.startpage2051en_US
dc.identifier.endpage2060en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US


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